HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethoxyethylamine → HCID 178467959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethoxyethylamine | HCID 66970 | — |
| Reactant | HCID 178426451 | HCID 178426451 | — |
| Product | HCID 178467959 | HCID 178467959 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 112 using 6-(4-(4-cyano-2-methylphenyl)-5-hydroxy-1H-pyrazol-1-yl)nicotinic acid and 2-ethoxyethylamine 1H NMR (400 MHz, DMSO-d6) δ ppm 1.12 (t, J=6.95 Hz, 3 H) 2.43 (s, 3 H) 3.42-3.49 (m, 4 H) 3.49-3.55 (m, 2 H) 7.66 (dd, J=8.08, 1.52 Hz, 1 H) 7.73 (s, 1 H) 7.75-7.85 (m, 1 H) 8.06-8.27 (m, 1 H) 8.42 (d, J=6.82 Hz, 2 H) 8.80 (t, J=5.18 Hz, 1 H) 8.88-8.96 (m, 1 H) 12.86-13.47 (m, 1 H). MS m/z [M+H]+ 392.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040522B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-2674518ae58c41bdb6c640743c2993fd |
| Source note | uspto-grants-2015_05 |