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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 579133Generated: October 30, 2026

1177279-31-0 → HCID 178462756, compound

https://huagongshe.com/reaction/579133

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1177279-31-0HCID 20070061—
ReactantHCID 178426451HCID 178426451—
ProductHCID 178462756HCID 178462756—

Reaction Steps

The title compound was prepared in a manner similar to Example 112 using 6-(4-(4-cyano-2-methylphenyl)-5-hydroxy-1H-pyrazol-1-yl)nicotinic acid and 1-ethyl,2,2-dimethylpiperazine. 1H NMR (400 MHz, ACETONITRILE-d3) δ ppm 0.79-1.20 (m, 9 H) 2.36-2.48 (m, 5 H) 2.59 (d, J=6.06 Hz, 2 H) 3.15 (br. s., 1 H) 3.44 (br. s., 2 H) 3.69 (br. s., 1H) 7.53-7.59 (m, 1 H) 7.60-7.63 (m, 1 H) 7.63-7.66 (m, 1 H) 7.75 (s, 1 H) 8.01 (br. s., 2H) 8.42 (br. s., 1 H); ESI-MS m/z [M+H]+ 445.3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09040522B2
Source datasetuspto-grants-2015_05
ORD IDord-8e3629f50c1e4451862b86bc4fcf91db
Source noteuspto-grants-2015_05