HuagongsheHuagongshe Chemistry Print Report · For research reference only
1177279-31-0 → HCID 178462756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1177279-31-0 | HCID 20070061 | — |
| Reactant | HCID 178426451 | HCID 178426451 | — |
| Product | HCID 178462756 | HCID 178462756 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 112 using 6-(4-(4-cyano-2-methylphenyl)-5-hydroxy-1H-pyrazol-1-yl)nicotinic acid and 1-ethyl,2,2-dimethylpiperazine. 1H NMR (400 MHz, ACETONITRILE-d3) δ ppm 0.79-1.20 (m, 9 H) 2.36-2.48 (m, 5 H) 2.59 (d, J=6.06 Hz, 2 H) 3.15 (br. s., 1 H) 3.44 (br. s., 2 H) 3.69 (br. s., 1H) 7.53-7.59 (m, 1 H) 7.60-7.63 (m, 1 H) 7.63-7.66 (m, 1 H) 7.75 (s, 1 H) 8.01 (br. s., 2H) 8.42 (br. s., 1 H); ESI-MS m/z [M+H]+ 445.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040522B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-8e3629f50c1e4451862b86bc4fcf91db |
| Source note | uspto-grants-2015_05 |