HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178428090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178428092 | HCID 178428092 | — |
| Product | HCID 178428090 | HCID 178428090 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 412 using 6-(4-(4-cyanophenyl)-5-hydroxy-1H-pyrazol-1-yl)-4-methylnicotinic acid and 1-methylpiperazine. 1H NMR (400 MHz, DMSO-d6) δ ppm 2.39 (s, 3 H) 2.82 (s, 3 H) 4.02 (br. s., 4 H) 4.56 (br. s., 4 H) 7.79 (d, J=8.59 Hz, 2 H) 8.12 (br. s., 2 H) 8.37 (s, 1 H) 8.59 (br. s., 2 H); ESI-MS m/z (M+H)+ calc'd for C22H22N6O2, 403.18; found 403.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040522B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-77599ed6139542449208fb092c302e96 |
| Source note | uspto-grants-2015_05 |