Sodium Methoxide → HCID 13742679, compound

HRID 579693Notes

Reaction equation

HRID 579693 reaction equation
[CH2:1]([NH:5][C:6]1[CH:11]=[C:10]2[O:12][CH2:13][O:14][C:9]2=[CH:8][C:7]=1[N+:15]([O-:17])=[O:16])[CH2:2][CH2:3][CH3:4].C[O-].[Na+]>CO>[CH3:13][O:12][C:10]1[CH:11]=[C:6]([NH:5][CH2:1][CH2:2][CH2:3][CH3:4])[C:7]([N+:15]([O-:17])=[O:16])=[CH:8][C:9]=1[OH:14]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 137426722-n-Butylamino-4,5-methylenedioxy-1-nitrobenzene

Product 1

HCID 13742679HCID 13742679, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A solution of 0.03 mol (6.9 g) of 2-n-butylamino-4,5-methylenedioxy-1-nitrobenzene, prepared according to Example 4, in 45 ml of a 30% strength solution of sodium methylate in methanol is brought for 15 minutes to the refluxing temperature of the methanol.

Sources & evidence

ORD record
ord-b13ddb2eaab84328bb0afb38784684e1
Source dataset
uspto-grants-1988_06
Patent number
US04749379

Reaction notes

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