Glycerol → HCID 13742681, compound

HRID 579695Notes

Reaction equation

[OH-].[K+].[CH2:3]([NH:7][C:8]1[CH:13]=[C:12]2[O:14][CH2:15][O:16][C:11]2=[CH:10][C:9]=1[N+:17]([O-:19])=[O:18])[CH2:4][CH2:5][CH3:6].[OH:20][CH2:21][CH:22](CO)[OH:23]>>[OH:20][CH:21]([CH2:22][OH:23])[CH2:15][O:14][C:12]1[CH:13]=[C:8]([NH:7][CH2:3][CH2:4][CH2:5][CH3:6])[C:9]([N+:17]([O-:19])=[O:18])=[CH:10][C:11]=1[OH:16]

Participants

Reactant 3

HCID 753Glycerol

HCID 14797Potassium Hydroxide

HCID 137426722-n-Butylamino-4,5-methylenedioxy-1-nitrobenzene

Product 1

HCID 13742681HCID 13742681, compound

Procedure

0.128 mol (8.5 g) of 85% pure potassium hydroxide pellets is dissolved in 70 ml of double-distilled glycerol on a boiling water bath. 2-n-butylamino-4,5-methylenedioxy-1-nitrobenzene, prepared according to Example 4, is added with stirring.

Workup

additionis added

Sources & evidence

ORD record: ord-68ed992602f14e1eb0a68f90279ed75e
Source dataset: uspto-grants-1988_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04749379

Reaction notes

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