Ethanol → HCID 13742683, compound

HRID 579696Notes

Reaction equation

HRID 579696 reaction equation
[OH-].[K+].[OH:3][CH2:4][CH2:5][NH:6][C:7]1[CH:12]=[C:11]2[O:13][CH2:14][O:15][C:10]2=[CH:9][C:8]=1[N+:16]([O-:18])=[O:17].[CH2:19](O)C>>[CH2:14]([O:13][C:11]1[CH:12]=[C:7]([NH:6][CH2:5][CH2:4][OH:3])[C:8]([N+:16]([O-:18])=[O:17])=[CH:9][C:10]=1[OH:15])[CH3:19]

Participants

4

Reactant 3

HCID 702EthanolHCID 14797Potassium HydroxideHCID 13742676HCID 13742676, compound

Product 1

HCID 13742683HCID 13742683, compound

Procedure

0.16 mol (10.5 g) of 85% pure potassium hydroxide pellets are dissolved in 80 ml of absolute ethanol on a boiling water bath. 0.08 mol (18.1 g) of 2-(β-hydroxyethyl)amino-4,5-methylenedioxy-1-nitrobenzene is added with stirring in the course of 10 minutes.

Sources & evidence

ORD record
ord-4392f711507849a2afe44b45612db4e4
Source dataset
uspto-grants-1988_06
Patent number
US04749379

Reaction notes

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