HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile → N-Benzylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile | HCID 7505 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Product | N-Benzylacetamide | HCID 11500 | — |
| Product | (Z)-Benzaldehyde oxime | HCID 12143 | — |
Reaction Steps
Also, by reaction of benzaldoxime with acetic anhydride benzaldoxime acetate is formed, which is then reduced, thus benzylamine being obtained with 91% (K. W. Rosenmund et al, Ber., 56 2258-2262 (1923)). These processes of reducing benzonitrile or benzaldoxime in the acetic anhydride solvent comprise isolating N-acetylbenzylamine and hydrolysing same to obtain benzylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04751328 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-68765ddf77944458a5757ad984f70f48 |
| Source note | uspto-grants-1988_06 |