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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 580175Generated: October 30, 2026

Hydrochloric Acid → HCID 20135764, compound

https://huagongshe.com/reaction/580175

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 13210613HCID 13210613—
SolventEthanolHCID 702—
ProductHCID 20135764HCID 20135764—

Reaction Steps

In 50 ml of absolute ethyl alcohol was dissolved 4.0 g of the 1-(3-piperidinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-piperidinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole dihydrochloride having the following analytical value.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04751302
Source datasetuspto-grants-1988_06
ORD IDord-4972874de93849e9b8d2704e0ae03569
Source noteuspto-grants-1988_06