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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 580183Generated: October 29, 2026

Hydrochloric Acid → HCID 20135900, compound

https://huagongshe.com/reaction/580183

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 13210625HCID 13210625—
SolventEthanolHCID 702—
ProductHCID 20135900HCID 20135900—

Reaction Steps

In 50 ml of absolute ethyl alcohol was dissolved 3.0 g of the 1-(3-morpholinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-morpholinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole dihydrochloride having the following analytical value.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04751302
Source datasetuspto-grants-1988_06
ORD IDord-e0b2e931e4c84d57867d8b62507d18ac
Source noteuspto-grants-1988_06