HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13849583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13849582 | HCID 13849582 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13849583 | HCID 13849583 | — |
Reaction Steps
The ester (1.0 g, 0.00266 mol) from Example 21 is stirred in 100 mL methanol and 10 mL 10% sodium hydroxide solution for 24 hours. Water (25 mL) is added and the methanol removed in vacuo. Acidification of the aqueous layer gives a brown precipitate which upon filtration and crystallization from methanol-water has mp 260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04752323 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-2cefe473328c401ab7c6cbece1f81949 |
| Source note | uspto-grants-1988_06 |