HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Bis(2-chloroethoxy)ethane → 1,4-Dioxa-7,10,13-trithiacyclopentadecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Bis(2-chloroethoxy)ethane | HCID 8171 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Bis(2-mercaptoethyl) sulfide | HCID 77117 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1,4-Dioxa-7,10,13-trithiacyclopentadecane | HCID 15918510 | — |
Reaction Steps
This compound is obtained by reacting 1,5-dimercapto-3-thiapentane with 1,8-dichloro-3,6-dioxaoctane in the presence of cesium carbonate in dimethylformamide (DMF): ##STR2##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04752560 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-9a9f2e69e5d948aa98b3cb162011c307 |
| Source note | uspto-grants-1988_06 |