Pyridine → HCID 13206463, compound

Participants

Reaction Steps

In 50 ml of toluene were dissolved 1.9 g (0.014 mole) of 2-methoxybenzylamine and 1.2 g (0.015 mole) of pyridine. Then, was added dropwise thereto a solution of 2.8 g (0.012 mole) of 2-(4-nitrophenoxy)-butyroyl chloride in 30 ml of toluene and the mixture was treated according to the same procedure as in Synthesis Example 7. The resultant crude crystals were recrystallized from ethanol to give 2.4 g of N-(2-methoxybenzyl)-2-(4-nitrophenoxy)-butyramide melting at 109°~112° C. as colorless needles.

Provenance & Evidence