HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-1-propanamine → HCID 13952758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | 5-Bromoisatoic Anhydride | HCID 288561 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13952758 | HCID 13952758 | — |
Reaction Steps
A mixture of 9.68 g of 5-bromoisatoic anhydride, 5.0 g of 1H-imidazol-1-propanamine and 75 ml of ethanol was stirred at room temperature for 20 hours and concentrated. The residue was washed onto a filter with ethanol and washed with ether for the desired product, mp 154°-156° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753944 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-1ef42539bb04410385e42ece62437f3b |
| Source note | uspto-grants-1988_06 |