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HRID580538

反应详情

EQUATION

反应方程式

HRID 580538 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C1C(=O)N(C)C(=O)N(C)C1=O
HCID593714

未命名化合物

结构：Cc1cc(Oc2ccc(N)cc2)nc(C(C)C)n1
HCID20133966

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2ccc(NC(=O)C3C(=O)N(C)C(=O)N(C)C3=O)cc2)nc(C(C)C)n1
HCID20133965

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

3.0 g (0.013 mole) of 1,3-dimethyl-5-ethoxycarbonylbarbituric acid and 3.2 g (0.013 mole) of 4-(2-isopropyl-6-methylpyrimidin-4-yloxy)aniline are suspended in 30 ml of toluene and heated for 18 hours at reflux temperature in an inert gas atmosphere (nitrogen). After cooling, the precipitate is isolated by filtration, washed with alcohol and dried.

WORKUP

后处理

  1. temperatureheated for 18 hours
  2. temperatureat reflux temperature in an inert gas atmosphere (nitrogen)
  3. temperatureAfter cooling
  4. customthe precipitate is isolated by filtration
  5. washwashed with alcohol
  6. customdried