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HRID580643

反应详情

EQUATION

反应方程式

HRID 580643 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccc(OCc2ccccc2)c(NS(C)(=O)=O)c1
HCID12363923

N-[5-Acetyl-2-(phenylmethoxy)phenyl]methanesulfonamide

C16H17NO4S

结构：CC(=O)c1ccc(OCc2ccccc2)c(CO)c1
HCID12969323

1-[3-(Hydroxymethyl)-4-(phenylmethoxy)phenyl]ethanone

C16H16O3

PRODUCTS

生成物

1
结构：CS(=O)(=O)Nc1cc(C(=O)C=O)ccc1OCc1ccccc1
HCID10042436

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO.O
溶剂HCID19096565

未命名化合物

PROCEDURE

实验过程

The compound was sbtained as an ethanol hemiacetal, mp 125°-128° (ethanol-water) by the process of Description 54 replacing 1-(4-benzyloxy-3-hydroxymethylphenyl)ethanone by 1-(4-benzyloxy-3-methanesulphonamidophenyl)ethanone. (CDCl3) 8.75 (3H, t, J=6 Hz), 7.05 (3H, s), 5.90-6.40 (2H, m), 4.90 (1H, b), 4.80 (2H, s), 4.46 (1H, s), 2.90 (1H, d, J=8 Hz), 2.60 (5H, s), 2.20 (1H, s), 2.09 (1H, dd, J=8 Hz, 2 Hz), 1.80 (1H, d, J=2 Hz).