HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14228262, compound → 2,1,3-Benzoxadiazole, 4,6-dichloro-, 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14228262 | HCID 14228262 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2,1,3-Benzoxadiazole, 4,6-dichloro-, 1-oxide | HCID 3623774 | — |
Reaction Steps
The compound 2,4-dichloro-6-nitroazidobenzene is dissolved in glacial acetic acid then refluxed for several hours to yield 4,6-dichlorobenzofuroxan. This step is similar to that described in Boulton et al., J. Chem. Soc. B., p. 909 (1967) except that the present invention uses a longer reflux time.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04754040 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-f141f173543d48a983c88186c796f03a |
| Source note | uspto-grants-1988_06 |