2-Chloropyridine → HCID 53870475, compound

HRID 580859Notes

Reaction equation

HRID 580859 reaction equation
Cl[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[OH:8][CH2:9][CH:10]1[O:15][CH2:14][CH2:13][NH:12][CH2:11]1>>[OH:8][CH2:9][CH:10]1[O:15][CH2:14][CH2:13][N:12]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=2)[CH2:11]1

Participants

3

Reactant 2

HCID 79772-ChloropyridineHCID 3497988Morpholin-2-ylmethanol

Product 1

HCID 53870475HCID 53870475, compoundYield 72%

Procedure

The title compound (33.0 g, 72%) was prepared as a thick liquid from 2-chloropyridine (54.32 g) and 2-hydroxymethyl morpholine (28.0 g) by a similar procedure to that described in preparation 1.

Workup

  1. customthat described in preparation 1

Sources & evidence

ORD record
ord-49bc1f68b67d40e8bf7a89e56bc45666
Source dataset
uspto-grants-1999_07
Patent number
US05919782

Reaction notes

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