HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 3,6-dihydro-2H-pyridin-1-yl(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Product | 3,6-dihydro-2H-pyridin-1-yl(phenyl)methanone | HCID 570037 | — |
Reaction Steps
Benzoyl chloride (60 mmole) is added to a solution of 38 (60 mmole) in pyridine at 4 C. The mixture is allowed to stir for about 1-2 hrs and then further stirred at room temp for 12 hrs. The reaction mixture is made acidic and then extracted with methylene chloride. Following work-up and flash chromatography affords 39.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05919797 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-8f31e158b4d14fca86080a938096478b |
| Source note | uspto-grants-1999_07 |