HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylvanillin → HCID 53859634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylvanillin | HCID 8467 | — |
| Reactant | HCID 53859634 | HCID 53859634 | — |
| Product | HCID 53859634 | HCID 53859634 | — |
| Product | HCID 54283220 | HCID 54283220 | — |
Reaction Steps
Ethyl-3-(3-allyl-4-trifluoromethylsulphonyloxyphenyl)propionate was prepared from ethyl vanillin using the procedure described in Example 1 for the preparation of ethyl 3-(3-allyl-4-trifluoromethylsulphonyloxyphenyl)propionate. Thus there was obtained 3-ethoxy-4-trifluoromethylsulphonyloxybenzaldehyde as an oil; NMR (CDCl3): 1.50(3H, t), 4.22(2H, q), 7.36-7.58(3H, m), 9.97(1H, s); m/Z 299 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05919793 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-02e450b53c524c979fb0b502cf538cdb |
| Source note | uspto-grants-1999_07 |