HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-{4-[(prop-2-en-1-yl)oxy]phenyl}propanoate → Methoxyethyl 2-methyl-3-(3-allyl-4-hydroxyphenyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-{4-[(prop-2-en-1-yl)oxy]phenyl}propanoate | HCID 19348971 | — |
| Reactant | Methoxyethyl 2-methyl-3-(4-allyloxyphenyl)propionate | HCID 54219826 | — |
| Reactant | Ethyl 3-[4-hydroxy-3-(prop-2-EN-1-YL)phenyl]propanoate | HCID 54533632 | — |
| Product | Methoxyethyl 2-methyl-3-(3-allyl-4-hydroxyphenyl)propionate | HCID 54051086 | — |
| Product | Methoxyethyl 2-methyl-3-(4-allyloxyphenyl)propionate | HCID 54219826 | — |
Reaction Steps
Methoxyethyl 2-methyl-3-(4-allyloxyphenyl)propionate was prepared using the procedure used to prepare ethyl 3-(4-allyloxyphenyl)propionate (see Example 1). Methoxyethyl 2-methyl-3-(3-allyl-4-hydroxyphenyl)propionate was prepared from methoxyethyl 2-methyl-3-(4-allyloxyphenyl)propionate using the method described in Example 1 for the preparation of ethyl 3-(3-allyl-4-hydroxyphenyl)propionate. The product was isolated as a yellow oil; microanalysis; found: C, 69.0 H, 7.70%; C16H22O4 requires C, 69.0 H. 7.97%; m/z 279 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05919793 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-09fd11bccb7940baaabbd169fd08c0c3 |
| Source note | uspto-grants-1999_07 |