HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl isocyanate → HCID 54223957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Reactant | 3-(1-Methyl-piperidin-4-yl)-1H-pyrrolo[3,2-b]pyridin-5-ylamine | HCID 10220230 | — |
| Product | HCID 54223957 | HCID 54223957 | 78.5% |
Reaction Steps
Beginning with 0.15 gm (0.65 mMol) 5-amino-3-(1-methylpiperidin-4-yl)pyrrolo[3,2-b]pyridine and 0.088 mL (0.78 mMol) butyl isocyanate, 0.168 gm (78%) of the title compound were recovered essentially by the procedure of Example 122. An analytical sample was crystallized from aqueous ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05919936 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-1d690e13792c4f989c6a2f419a26fc86 |
| Source note | uspto-grants-1999_07 |