HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus sulfide (P2S5) → 3-Methylquinoxaline-2-thiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | HCID 178418588 | HCID 178418588 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3-Methylquinoxaline-2-thiol | HCID 178418627 | — |
Reaction Steps
2-Hydroxy-3-methylquinoxaline (2 g) and phosphorus pentasulphide (3.05 g) were stirred together in 40 ml of pyridine and the reaction mixture heated to reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05246933 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-7070d8bc971546909aeafe6e08288d5c |
| Source note | uspto-grants-1993_09 |