1-Benzylpiperidine → HCID 86754204, compound

HRID 581738Notes

Reaction equation

HRID 581738 reaction equation
Cl[CH2:2][CH2:3][CH2:4][S:5][C:6]1[CH:11]=[CH:10][N:9]=[C:8]([CH2:12][S:13][C:14]2[NH:18][C:17]3[CH:19]=[CH:20][CH:21]=[CH:22][C:16]=3[N:15]=2)[C:7]=1[O:23][CH3:24].[CH2:25](N1CCCCC1)[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[CH2:25]([CH:6]1[CH2:11][CH2:10][N:9]([CH2:2][CH2:3][CH2:4][S:5][C:6]2[CH:11]=[CH:10][N:9]=[C:8]([CH2:12][S:13][C:14]3[NH:18][C:17]4[CH:19]=[CH:20][CH:21]=[CH:22][C:16]=4[N:15]=3)[C:7]=2[O:23][CH3:24])[CH2:8][CH2:7]1)[C:26]1[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 761901-BenzylpiperidineHCID 54054490HCID 54054490, compound

Product 1

HCID 86754204HCID 86754204, compound

Procedure

According to the procedure indicated in Example 1), reaction of 2-{[[4-(3-chloropropylthio)-3-methoxy-2-pyridinyl]methyl]thio}-1H-benzimidazole with N-benzylpiperidine gives the title compound; beige powder; m.p. 73-75° C. (hydrated).

Sources & evidence

ORD record
ord-30d29a2c1fef469688a09dab1d8bc242
Source dataset
uspto-grants-1999_07
Patent number
US05922720

Reaction notes

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