HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N1-Benzyl-N2-phenylethane-1,2-diamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Benzenemethanamine, N-(2-chloroethyl)-, hydrochloride (1:1) | HCID 13054189 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N1-Benzyl-N2-phenylethane-1,2-diamine hydrochloride | HCID 12366334 | — |
Reaction Steps
A solution of 13 (8.618 g, 42.0 mmol) and aniline (11.75 g, 126 mmol) in toluene (40 niL) was heated to 130° C. (1.5 h). The mixture was triturated with dichloromethane (200 mL) and filtered. Recrystallization from ethanol (220 mL) afforded the title compound 14 as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922722 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-5d57463423324e5d98f7f4f2427b6858 |
| Source note | uspto-grants-1999_07 |