Ethylamine → HCID 86750054, compound

Participants

Reaction Steps

A solution of 3-pyridinecarboxaldehyde (1 g, 9.3 mmol) and ethylamine (661 mg, 10.2 mmol, 70% wt in water) was strirred at room temperature for 18 h. The reaction mixture was diluted with chloroform (20 mL) and dried over anhydrous K2CO3. The solution was filtered and the solvent was evaporated to afford N-(3-pyridylidene)-ethylamine (XVII) 1.15 g (92%), which was used immediately without further purification. 1H NMR (CDCl3): δ 8.82 (s, 1H), 8.60 (d, 1H), 8.28 (s,1H), 8.10 (m, 1H), 7.4-7.3 (m, 1H), 3.78-3.62 (q, 2H), 1.38-1.22 (t, 3H).

Provenance & Evidence