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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 581848Generated: October 31, 2026

Pyridine → HCID 86754218, compound

https://huagongshe.com/reaction/581848

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant4-Toluenesulfonyl chlorideHCID 7397—
ReactantCyclopent-3-en-1-ylmethanolHCID 1514122—
ProductHCID 86754218HCID 8675421883.2%

Reaction Steps

A mixture of (cyclopent-3-en-1-yl)methanol (1.96 g, 20 mmol) and para-toluenesulfonylchloride (3.81 g, 20 mmol) were stirred at room temperature for 2 hrs in pyridine (30 ml). After the concentration of pyridine, the reaction residues were extracted with dichloromethane, washed 1N HCl, dried with MgSO4, concentrated and separated by the column chromatography to give the desirable product (4.20 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05922727
Source datasetuspto-grants-1999_07
ORD IDord-82c9268c62c04cfea2182649ff42a46c
Source noteuspto-grants-1999_07