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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 581851Generated: November 2, 2026

Pyridine → HCID 88084319, compound

https://huagongshe.com/reaction/581851

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant4-Toluenesulfonyl chlorideHCID 7397—
Reactant1-Cyclopentene-1-methanolHCID 11051584—
ProductHCID 88084319HCID 8808431989.6%

Reaction Steps

A mixture of (cyclopent-1-en-1-yl)methanol (1.96 g, 20 mmol) and para-toluenesulfonylchloride (3.81 g, 20 mmol) were stirred at room temperature for 2 hrs in pyridine (30 ml). After the concentration of pyridine, the reaction residues were extracted with dichloromethane, washed 1N HCl, dried with MgSO4, concentrated and separated by the column chromatography to give the desirable product (4.52 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05922727
Source datasetuspto-grants-1999_07
ORD IDord-752adc126ed945b7b6087687603e2034
Source noteuspto-grants-1999_07