HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(3,5-dimethylphenyl)sulfanyl-5-ethyl-1H-pyrimidine-2,4-dione → 1-[(5-Hydroxymethylcyclopent-1-en-1-yl) methyl]-5-ethyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(3,5-dimethylphenyl)sulfanyl-5-ethyl-1H-pyrimidine-2,4-dione | HCID 10492727 | — |
| Reactant | (5-t-Butyldimethylsilyloxymethylcyclopent-1-en-1-yl)methyl bromide | HCID 53795506 | — |
| Product | 1-[(5-Hydroxymethylcyclopent-1-en-1-yl) methyl]-5-ethyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione | HCID 54314278 | 22.7% |
Reaction Steps
5-Ethyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione and (5-t-butyldimethylsilyloxymethylcyclopent-1-en-1-yl)methyl bromide were reacted by the same with the example 10 to obtain the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922727 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-7a3eda18d41c4f37ada165513028503c |
| Source note | uspto-grants-1999_07 |