HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione → 6-(3,5-Dimethylphenoxy)-5-ethyl-1-[[5-(hydroxymethyl)cyclopenten-1-yl]methyl]pyrimidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione | HCID 10923266 | — |
| Reactant | (5-t-Butyldimethylsilyloxymethylcyclopent-1-en-1-yl)methyl bromide | HCID 53795506 | — |
| Product | 6-(3,5-Dimethylphenoxy)-5-ethyl-1-[[5-(hydroxymethyl)cyclopenten-1-yl]methyl]pyrimidine-2,4-dione | HCID 474600 | 21.3% |
Reaction Steps
5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione and (5-t-butyldimethylsilyloxymethylcyclopent-1-en-1-yl)methyl bromide were reacted by the same method with example 6 to obtain the titled compound (52 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922727 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-ab75203508ce461ba4244e0c6df38820 |
| Source note | uspto-grants-1999_07 |