HCID 86754222, compound → HCID 69978190, compound

HRID 581890Notes

Reaction equation

HRID 581890 reaction equation
[CH:1]([C:4]1[C:5](=[O:21])[NH:6][C:7](=[O:20])[NH:8][C:9]=1[C:10](=[O:19])[C:11]1[CH2:12][C:13](=[CH2:18])[CH2:14][C:15](=[CH2:17])[CH:16]=1)([CH3:3])[CH3:2].C1(C)C(S(O[CH2:32][CH2:33][CH:34]2[CH2:38][CH2:37][CH2:36][CH2:35]2)(=O)=O)=CC=CC=1>>[CH2:35]1[CH2:36][CH2:37][CH2:38][CH:34]1[CH:33]([N:8]1[C:9]([C:10](=[O:19])[C:11]2[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=2)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:21])[NH:6][C:7]1=[O:20])[CH3:32]

Participants

3

Reactant 2

HCID 86754222HCID 86754222, compoundHCID 131721306HCID 131721306, compound

Product 1

HCID 69978190HCID 69978190, compoundYield 24.9%

Procedure

5-Isopropyl-6-(3,5-dimethlylbenzoyl)-2,4-pyrimidinedione and (2-cyclopentyl)ethyl toluenesulfonate were reacted by the same method with example 44 to obtain the titled compound (95 mg).

Sources & evidence

ORD record
ord-edb4828faee2480bacbb2a71ed90622f
Source dataset
uspto-grants-1999_07
Patent number
US05922727

Reaction notes

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