HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 86754224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 5-Formyl-1-(3-(4-pyrimidyl)phenyl)benzimidazole | HCID 53950824 | — |
| Product | HCID 86754224 | HCID 86754224 | 76.1% |
Reaction Steps
was synthesized as described in Example 22 using (62) (150 mg, 0.50 mmol) instead of (55) and NH2OH.HCl (100 mg, 1.5 mmol). The reaction gave (63) (120 mg, 76%).Mp. 220-221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922725 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-8c9e31d3d8b744859d2ccf943ce9fc73 |
| Source note | uspto-grants-1999_07 |