3-(2-Pyridyl)aniline → N-(3-(2-Pyridyl)phenyl)-4-iodo-2-nitroaniline

HRID 581937Notes

Reaction equation

HRID 581937 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([I:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[N:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[C:18]1[CH:19]=[C:20]([CH:22]=[CH:23][CH:24]=1)[NH2:21]>>[N:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[C:18]1[CH:19]=[C:20]([NH:21][C:2]2[CH:7]=[CH:6][C:5]([I:8])=[CH:4][C:3]=2[N+:9]([O-:11])=[O:10])[CH:22]=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 4595173-(2-Pyridyl)anilineHCID 145905821-Fluoro-4-iodo-2-nitrobenzene

Product 1

HCID 53888257N-(3-(2-Pyridyl)phenyl)-4-iodo-2-nitroanilineYield 40%

Procedure

N-(3-(2-Pyridyl)phenyl)-4-iodo-2-nitroaniline (6f) was prepared analogously from 1c (Example 1) and 2f (Example 4). Yield: 40%. Mp 195-196° C.

Sources & evidence

ORD record
ord-62574a15394f484dadfd5d8c8153a456
Source dataset
uspto-grants-1999_07
Patent number
US05922724

Reaction notes

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