Furan-3-boronic acid → HCID 54102656, compound

HRID 581940Notes

Reaction equation

HRID 581940 reaction equation
[N:1]1([C:6]2[CH:7]=[C:8]([NH:12][C:13]3[CH:18]=[CH:17][C:16]([N+]([O-])=O)=[CH:15][C:14]=3[N+:22]([O-:24])=[O:23])[CH:9]=[CH:10][CH:11]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1.[O:25]1[CH:29]=[CH:28][C:27](B(O)O)=[CH:26]1>>[N:1]1([C:6]2[CH:7]=[C:8]([NH:12][C:13]3[CH:18]=[CH:17][C:16]([C:27]4[CH:28]=[CH:29][O:25][CH:26]=4)=[CH:15][C:14]=3[N+:22]([O-:24])=[O:23])[CH:9]=[CH:10][CH:11]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 2734358Furan-3-boronic acidHCID 54379348HCID 54379348, compound

Product 1

HCID 54102656HCID 54102656, compoundYield 86%

Procedure

N-(3-(1-Pyrrolyl)phenyl)-4-(3-furanyl)-2-nitroaniline (7k) was prepared analogously from 6k (Example 9) and 3-furanylboronic acid. Yield: 86%. Mp 129-131° C.

Sources & evidence

ORD record
ord-ced0fcd6e6e44589b14cd5fc8e229075
Source dataset
uspto-grants-1999_07
Patent number
US05922724

Reaction notes

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