Furan-2-boronic acid → HCID 53713614, compound

HRID 581943Notes

Reaction equation

HRID 581943 reaction equation
F.[NH2:2][C:3]1[N:8]=[CH:7][C:6]([C:9]2[CH:10]=[C:11]([NH:15][C:16]3[CH:21]=[CH:20][C:19](I)=[CH:18][C:17]=3[N+:23]([O-:25])=[O:24])[CH:12]=[CH:13][CH:14]=2)=[CH:5][N:4]=1.[O:26]1[CH:30]=[CH:29][CH:28]=[C:27]1B(O)O>>[NH2:2][C:3]1[N:8]=[CH:7][C:6]([C:9]2[CH:10]=[C:11]([NH:15][C:16]3[CH:21]=[CH:20][C:19]([C:27]4[O:26][CH:30]=[CH:29][CH:28]=4)=[CH:18][C:17]=3[N+:23]([O-:25])=[O:24])[CH:12]=[CH:13][CH:14]=2)=[CH:5][N:4]=1

Participants

3

Reactant 2

HCID 2734357Furan-2-boronic acidHCID 67482348HCID 67482348, compound

Product 1

HCID 53713614HCID 53713614, compound

Procedure

N-(3-(2-Aminopyrimid-5-yl)phenyl)-4-(2-furanyl)-2-nitroaniline (7p) was prepared analogously from 6l (Example 10) and 2-furanylboronic acid in quantitative yield. Mp 178-180° C.

Sources & evidence

ORD record
ord-663482c533cc410f9fe71b229dc25689
Source dataset
uspto-grants-1999_07
Patent number
US05922724

Reaction notes

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