HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12776873, compound → HCID 54559694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12776873 | HCID 12776873 | — |
| Reactant | HCID 53704157 | HCID 53704157 | — |
| Product | HCID 54559694 | HCID 54559694 | — |
Reaction Steps
The title compound was prepared by adding (3-methyl-4-chlorophenylthio)acetaldehyde diethyl acetal to polyphosphoric acid under reduced pressure (1.5 mm Hg).* This gave 1.8 g of a mixture of the title compound (D27) and 4-methyl-5-chlorobenzo[b]thiophene in a 60:40 ratio.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922733 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-1d8cabcf1a494199ae0d0b959803cd64 |
| Source note | uspto-grants-1999_07 |