HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 70347532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 3-(4-methylsulfonylphenyl)-2-pyridin-3-ylcyclopent-2-en-1-one | HCID 9796843 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70347532 | HCID 70347532 | — |
Reaction Steps
To a solution of 3-(4-(methylsulfonyl)phenyl)-2-(3-pyridinyl)-2-cyclopenten-1-one (104 mg, 0.33 mmol) in CH2Cl2 (50 mL) was added methanesulfonic acid (0.02 mL, 0.32 mmol) and the solution was concentrated to give a foam. The foam was swished in Et2O to give 108 mg of the title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922742 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-697858c0522c491ab9514852bd45054b |
| Source note | uspto-grants-1999_07 |