Acetonitrile → HCID 11044017, compound
Reaction equation
[CH2:1]([CH:8]1[CH2:16][C:15]2[C:10](=[CH:11][C:12]([O:17][CH3:18])=[CH:13][CH:14]=2)[C:9]1=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:20](#[N:22])[CH3:21]>>[CH2:1]([CH:8]1[CH2:16][C:15]2[C:10](=[CH:11][C:12]([O:17][CH3:18])=[CH:13][CH:14]=2)/[C:9]/1=[CH:21]/[C:20]#[N:22])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
Starting with 2-benzyl-6-methoxy-1-indanone and acetonitrile, the title compound was synthesized in otherwise the same manner as Reference Example 1 (yield 76%). This compound was used in the next reaction without further purification.
Workup
- customThis compound was used in the next reaction without further purification
Sources & evidence
- ORD record
- ord-dd2a94325abf4a45951fbc7449f1e0af
- Source dataset
- uspto-grants-1999_07
- Patent number
- US05922771
Reaction notes
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