Acetyl chloride → HCID 54143275, compound
Reaction equation
Cl.[Br:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7]([CH2:12][CH2:13][NH2:14])=[CH:8][CH2:9]2)=[CH:5][C:4]=1[O:15][CH3:16].[C:17](Cl)(=[O:19])[CH3:18]>>[Br:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7]([CH2:12][CH2:13][NH:14][C:17](=[O:19])[CH3:18])=[CH:8][CH2:9]2)=[CH:5][C:4]=1[O:15][CH3:16]Participants
3
Procedure
Starting with 2-(6-bromo-5-methoxy-1H-inden-3-yl)ethylamine hydrochloride and acetyl chloride, the title compound was synthesized in otherwise the same manner as Example 8 (yield 83%).
Sources & evidence
- ORD record
- ord-4da30d5780c34dd0a18e28aca66c89b9
- Source dataset
- uspto-grants-1999_07
- Patent number
- US05922771
Reaction notes
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