HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanediamine, N1,N1,N2-trimethyl- → HCID 53672891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanediamine, N1,N1,N2-trimethyl- | HCID 67338 | — |
| Reactant | 4-[1-[3-(Isopropylamino)-2-pyridyl]piperazin-4-yl-carbonyl]benzoic acid | HCID 10959558 | — |
| Product | HCID 53672891 | HCID 53672891 | 80% |
Reaction Steps
By the same procedure as described in the example 46, synthesis was carried out starting with 4-[1-[3-(isopropylamino)-2-pyridyl]piperazin-4-yl-carbonyl]benzoic acid and using N,N,N'-trimethylethylenediamine. Then, the product was recrystallized using isopropanol and ether to give the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922871 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-363ee843fba04f73ba22e71923eac50e |
| Source note | uspto-grants-1999_07 |