HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → 2-(2-Methacryloyloxyethoxy)ethyl-dimethylethylammonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | 2-(2-Dimethylaminoethoxy)ethyl Methacrylate | HCID 15870290 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-(2-Methacryloyloxyethoxy)ethyl-dimethylethylammonium bromide | HCID 86754240 | — |
Reaction Steps
2-(2-dimethylaminoethoxy)ethyl methacrylate (8 g) was dissolved in acetone (20 g) and small amounts of hydroquinone (approx. 0.1 g) was added followed by the addition of bromoethane (8 g). The mixture was stirred at room temperature for 24 hours and the solvent was removed under reduced pressure at 25° C. Product was obtained as an amorphous solid. Yield 12.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925253 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-682bc4e213364f99940c656344af934d |
| Source note | uspto-grants-1999_07 |