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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 582585Generated: October 30, 2026

HCID 21993065, compound → HCID 15789650, compound

https://huagongshe.com/reaction/582585

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21993065HCID 21993065—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 15789650HCID 1578965076.2%

Reaction Steps

A solution of 2.09 g (6.1 mmol) of N-tert-butyl-5-acetamidomethyl-2-methoxycarbonylbenzenesulfonamide in 25 ml of trifluoroacetic acid is stirred at room temperature for 14 h and then evaporated to dryness. Crystallization of the residue from ethyl acetate yields 1.33 g (76%) of 5-acetamidomethyl-2-methoxycarbonylbenzenesulfonamide of mp. 173-175° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05925597
Source datasetuspto-grants-1999_07
ORD IDord-dca6efe07ced44948b2ec41e1b2996b4
Source noteuspto-grants-1999_07