N-Benzyl-N-methylethanolamine → HCID 54221496, compound
Reaction equation
[CH2:1]([N:8]([CH2:10][CH2:11][OH:12])[CH3:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.F[C:14]1[CH:21]=[CH:20][C:17]([CH:18]=[O:19])=[CH:16][CH:15]=1>>[CH2:1]([N:8]([CH2:10][CH2:11][O:12][C:14]1[CH:21]=[CH:20][C:17]([CH:18]=[O:19])=[CH:16][CH:15]=1)[CH3:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
The title compound was prepared from 2-(N-benzyl-N-methylamino)ethanol (2.5 g) obtained in example 8 and 4-fluorobenzaldehyde (2 ml) by an analogous procedure to that described in preparation 23.
Workup
- customthat described in preparation 23
Sources & evidence
- ORD record
- ord-26ad7549ce0f42b8bac7ed37c2e34c94
- Source dataset
- uspto-grants-1999_07
- Patent number
- US05925656
Reaction notes
Loading…