HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethyl-3-cyclopenten-1-ol → (1RS,4RS)-4-allyl-4-hydroxy-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethyl-3-cyclopenten-1-ol | HCID 13507601 | — |
| Reactant | (1RS,4RS)-4-allyl-4-methoxymethyl-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether | HCID 57275069 | — |
| Product | (1RS,4RS)-4-allyl-4-hydroxy-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether | HCID 57172708 | 92% |
Reaction Steps
From 4.50 g of (1RS,4RS)-4-allyl-4-hydroxy-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether was obtained by the same procedures as in (3) of the intermediate preparation example 1 (1RS,4RS)-4-allyl-4-methoxymethyl-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether in an amount of 4.88 g. Yield 92%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925676 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-6a3c78a01a104b619277098765c70321 |
| Source note | uspto-grants-1999_07 |