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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 582749생성일: 2026년 10월 25일

3,4-Dimethyl-3-cyclopenten-1-ol → (1RS,4RS)-4-hydroxy-4-(3-trimethylsilyl-2-propynyl)-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether

https://huagongshe.com/reaction/582749

반응식

참여 물질

역할이름HCID투입량
반응물3,4-Dimethyl-3-cyclopenten-1-olHCID 13507601—
반응물(1RS,4RS)-4-methoxymethoxy-4-(3-trimethylsilyl-2-propynyl)-2-cyclopenten-1-yl (t-butyldimethylsilyl) etherHCID 56993888—
생성물(1RS,4RS)-4-hydroxy-4-(3-trimethylsilyl-2-propynyl)-2-cyclopenten-1-yl (t-butyldimethylsilyl) etherHCID 8675428065%

반응 단계

From 8.9 g of (1RS,4RS)-4-hydroxy-4-(3-trimethylsilyl-2-propynyl)-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether was obtained by the same procedures as in (3) of the intermediate preparation example 1 (1RS,4RS)-4-methoxymethoxy-4-(3-trimethylsilyl-2-propynyl)-2-cyclopenten-1-yl (t-butyldimethylsilyl) ether in an amount of 6.6 g. Yield 65%

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05925676
출처 데이터셋uspto-grants-1999_07
ORD IDord-25cac8c3ae964aff932dbc08f8717973
출처 메모uspto-grants-1999_07