HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 54149707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 57131418 | HCID 57131418 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54149707 | HCID 54149707 | 38% |
Reaction Steps
By using 0.85 g of (RS)-3-(3-trimethylsilyl-2-propynyl)-3-cyclopenten-1-yl (t-butyldimethylsilyl) ether and 8.5 ml of 1 M tetrahydrofuran solution of tetrabutylammonium fluoride and by the same procedures as in (5) of the intermediate preparation example 1, there was obtained 128 mg of (RS)-3-propargyl-3-cyclopenten-1-ol. Yield 37%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925676 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-67bcb3d037594f9bb8556795d44c3d4d |
| Source note | uspto-grants-1999_07 |