HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldiphenylchlorosilane → Tert-butyl(cyclopent-3-en-1-yloxy)diphenylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldiphenylchlorosilane | HCID 94078 | — |
| Reactant | 3-Cyclopenten-1-ol | HCID 281478 | — |
| Product | Tert-butyl(cyclopent-3-en-1-yloxy)diphenylsilane | HCID 11347853 | 97% |
Reaction Steps
By using 2.2 g of 3-cyclopentenol prepared according to the method described in J. Org. Chem., 25, 26-29 (1960) and 9.2 g of t-butyldiphenylsilyl chloride and by the same procedures as in (1) of the intermediate preparation example 1, there was obtained 8.15 g of 3-cyclopenten-1-yl (t-butyldiphenylsilyl) ether. Yield 97%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925676 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-7773062c77624862afb02fc4a00ea9f1 |
| Source note | uspto-grants-1999_07 |