Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | SR142948A | HCID 5311451 | — |
| Reactant | HCID 178418600 | HCID 178418600 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178491337 | HCID 178491337 | 43.9% |
Reaction Steps
0.1 g of the compound obtained in EXAMPLE 1' and 0.03 g of (S)-(+)-arginine are dissolved in the heated state in 4 ml of MeOH, and this solution is concentrated to 1 ml and poured into 10 ml of ether cooled to 5° C. 0.055 g of the expected product is obtained after draining and drying over P2O5, m.p.=176° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05925661 |
|---|
| Source dataset | uspto-grants-1999_07 |
|---|
| ORD ID | ord-f0c9d091fd4c4411a273b17466d68ea3 |
|---|
| Source note | uspto-grants-1999_07 |
|---|
