HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5,6-Dichloronicotinate → Dimethyl 3-Chloro-2,6-pyridinedicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5,6-Dichloronicotinate | HCID 2782166 | — |
| Reactant | 2,3-Dichloro-5-(methoxymethyl)pyridine | HCID 11137960 | — |
| Product | Dimethyl 3-Chloro-2,6-pyridinedicarboxylate | HCID 53845654 | 73% |
Reaction Steps
Example 2 was repeated, except that the 2,3-dichloro-5-(methoxymethyl)pyridine was replaced by the same molar amount of methyl 2,3-dichloro-5-pyridinecarboxylate. After a reaction time of 6 hours at a bath temperature of 160° C., 1.20 g (73 percent) of a yellow product was obtained. Other data concerning the product was:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925765 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-09075152a86f4f358289b2225de3bb1c |
| Source note | uspto-grants-1999_07 |