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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 583261Generated: October 29, 2026

HCID 21584334, compound → HCID 21584263, compound

https://huagongshe.com/reaction/583261

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21584334HCID 21584334—
SolventMethanolHCID 887—
ProductHCID 21584263HCID 21584263103.6%

Reaction Steps

2-Nitro-6,6a,7,8,9,10-hexahydro-12H-pyrido[2,1-c][1,4]benzoxazepine hydrochloride (2.46 g) dissolved in methanol (50 ml) was treated with 10% Pd--C (0.25 g), and hydrogenated on a Parr Hydrogenator for one hour, filtered and evaporated to yield a tacky solid (2.28 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05929085
Source datasetuspto-grants-1999_07
ORD IDord-38fb9e0f6f94442886a040a0c91c4610
Source noteuspto-grants-1999_07