HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21584334, compound → HCID 21584263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21584334 | HCID 21584334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21584263 | HCID 21584263 | 103.6% |
Reaction Steps
2-Nitro-6,6a,7,8,9,10-hexahydro-12H-pyrido[2,1-c][1,4]benzoxazepine hydrochloride (2.46 g) dissolved in methanol (50 ml) was treated with 10% Pd--C (0.25 g), and hydrogenated on a Parr Hydrogenator for one hour, filtered and evaporated to yield a tacky solid (2.28 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929085 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-38fb9e0f6f94442886a040a0c91c4610 |
| Source note | uspto-grants-1999_07 |