HCID 54136701, compound → HCID 70053518, compound

HRID 583317Notes

Reaction equation

HRID 583317 reaction equation
[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[CH:8][C:7]([Cl:10])=[C:6]([CH3:11])[C:5]=1[NH:12][S:13]([C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1)(=[O:15])=[O:14]>CCCCCC>[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[CH:8][C:7]([Cl:10])=[C:6]([CH3:11])[C:5]=1[N:12]([CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[S:13]([C:16]1[CH:17]=[CH:18][C:19]([O:22][CH3:23])=[CH:20][CH:21]=1)(=[O:15])=[O:14]

Participants

3

Reactant 1

HCID 54136701HCID 54136701, compound

Product 1

HCID 70053518HCID 70053518, compoundYield 182.3%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

In the same manner as described in Example 9, 0.5 g (1.35 mmol) of the product of Example 96 provided 0.566 g (80%) of the desired product as a white solid after trituration with hexane. Electrospray Mass Spec 460.2(M+H).

Sources & evidence

ORD record
ord-c003bde233f04b8f8907c913ce778430
Source dataset
uspto-grants-1999_07
Patent number
US05929097

Reaction notes

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